Vogel's Textbook of Practical Organic Chemistry, Including Qualitative Organic AnalysisLongman, 1978 - 1368 páginas 1. Experimental techniques 1; 2. Solvents and reagents 264; 3. Aliphatic compounds 320; 4. Aromatic compounds 599; 5. Some alicyclic compounds 850; 6. Some heterocyclic compounds 873; 7. Qualitative organic analysis 931; 8. Physical constants of organic compounds 1158. |
Conteúdo
Apparatus and reaction procedures | 24 |
9 | 35 |
I12 | 44 |
Direitos autorais | |
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1-litre alcohol alkyl amine anhydride anhydrous anhydrous calcium apparatus aqueous beaker benzene boiling point bromide Buchner funnel calcium chloride carbon catalyst chromatography Cognate preparation Collect compounds concentrated hydrochloric acid concentrated sulphuric acid containing copper(I crude crystals decolourising diethyl dilute Dissolve distil the residue dropping funnel ester ethanol ether extract filter filter-paper filtrate fractionating column fume cupboard glass H₂O halide heat hydrochloric acid hydrogen ketone laboratory layer light petroleum liquid magnesium sulphate mechanical stirrer melting point methyl minutes ml of concentrated ml of water ml portions mmHg nitrogen obtained organic oxide potassium powdered procedure pump pure reaction mixture reagent recrystallisation redistilled reduced pressure reflux condenser remove room temperature rotary evaporator round-bottomed flask salt Section separate separatory funnel shaking sodium hydroxide sodium hydroxide solution solid solvent steam distillation stirring stopper suitable sulphuric acid three-necked flask toluene tube vapour vigorous wash water bath yield